This equipment is composed of electric constant speed stirring system, condensation, dropping system and heating bath. While stirring the materials, the bath heats the materials in the kettle. The evaporation efficiency can be increased under vacuum conditions ( a vacuum device need to be connected). The solvent vapor is cooled into liquid when passing through the glass condensing coil (a cooling device need to be connected), which can be refluxed into the kettle. It can also be recycled in collection flask.
This series of products need to be equipped with a vacuum device, a cooling circulating device, etc. to form a system devices.
Single Layer Glass Reactor Features:
The parts in contact with the material are all made of high borosilicate glass (expansion coefficient 3.3) and PTFE materials, which have stable performance and are not easy to react with the materials.
The main stent is made of cold plate anti-corrosive spray + aluminum alloy. And the bath is made of stainless steel.
ON-OFF tilt switch to control stirring and heating.
Electronic stepless speed regulation, fine-adjustment through knobs, speed box digital displaying speed.
Constant temperature bath with temperature digital display, K-type sensor at bottom of bath + stainless steel probe.
The stirring system uses ceramic bearings and mechanical seal to prevent the stirring rod from wearing out.
Vacuum pressure gauge shows real-time vacuum indicated by pointer.
Crescent-type stirring paddle, 304 stainless steel + PTFE stirring blade. The material of the stirring rod is 304 stainless steel, and it is wrapped in PTFE tube outside.
Stirring, heating two fuses safety protection.
Single Layer Glass Reactor Specifications:
| Model | GR-5L |
|---|
| Reactor volume | 5L spherical shape |
| Voltage/Frequency | 220V 50HZ/110V 60Hz |
| Stirring motor power | 90W |
| Heating power | 2KW |
| Stirring speed | 0-800rpm/min |
| Reactor temperature range | -80℃~ +250℃ |
| Temperature measuring accuracy | ±1℃ |
| Vacuum | 0.098Mpa |
Kettle body Φ230mm 5 ports | Stirring port | Φ50mm flange port |
| Condensation reflux port | 29# standard port |
| Port of constant pressure funnel | 29# standard port |
| Pressure relief port | 24# standard port |
| Temperature measuring port | 24# standard port |
| Stirring paddle | Φ10×530H(mm) blade 90mm |
| Condenser | Φ60mm×450H(mm); upper 24#standard port, lower 29#standard stopper |
| Constant pressure funnel | 500ml; upper 24#standard port with glass stopper, lower 29#standard stopper |
| Pressure relief valve | 24#Standard plug valve, air outlet (pagoda joint) with 10mm outer diameter |
| Temperature measuring port | 24#Standard stopper with glass temperature measuring tube |
| Collection device | Two adapters, 24# standard port 500 spherical collection flask |
| Vacuum nozzle | 24#Glass nozzle (pagoda joint) with 10mm outer diameter |
| In and out circulating nozzle of condenser coil | Pagoda joint with 10mm outer diameter |
| Bath size | Φ280×170H(mm) |
| Overall size(WxDxH)(mm) | (430-1030)×330×1150 |
| Net weight | 25KG |
| Packing size | 1020×480×520mm wooden package 0.26m³ |
| Packing weight | 40KG |
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